ASA a fourth out appeal may only be made on a runner who has scored, so no this would not be a valid appeal in ASA.
The fourth out appeal rule in NFHS does allow for 4th out appeals on any runner, but it speaks in reference to negating runs. In the situation you have presented it is not to negate a run so not sure that would be a valid 4th out appeal, but I am not sure.
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